Publications récentes

Publications et travaux récents

(depuis 2000)

Lien vers les articles soumis ou acceptés	Lien vers les thèses et mémoires
Lien vers les articles publiés	Communications orales
Communications par affiches	Lien vers les activités de recherche

Pour voir les abstracts, cliquer sur le nom de l'article (bleu et italique)
Pour télécharger les articles (rouge), veuillez prendre contact avec Francis Masin

Nanotube type (8,2); chiral et métallique

Articles soumis ou acceptés :

Solid state NMR study of the C-F bonding in highly fluorinated fullerenes
W. Zhang, M. Dubois, K. Guérin, P. Bonnet, D. Claves, H. Kharbache, F. Masin, A.P. Kharitonov, A. Hamwi,
Physical Chemistry, Chemical Physics
New synthesis methods for fluorinated carbon nanofibres and applications
W. Zhang, L. Spinelle, M. Dubois, K. Guérin, H. Kharbache, F. Masin, A.P. Kharitonov, A. Hamwi, J. Brunet, C. Varenne, A. Pauly, P. Thomas, D. Himmel, J. L. Mansot, Journal Fluorine Chemistry
Investigation of dynamics and characterization of Poly(Di-n-propylsiloxane) (PDPS) by Solid State 1H, 13C and 29Si NMR
J. Giraudet, A. Walter, P. Pirotte, D.A. Ivanov, F. Masin
Macromolecules
Fluorinated nanocarbons using fluorinating agent: Strategies of fluorination and applications
W. Zhang, M. Dubois, K. Guérin, P. Bonnet, A. Hamwi, J. Giraudet, F. Masin,
European Phys. J. B, F.I.: 1,5680, 9999, L. Colombo, A. Loidl and F. Schweitzer
Effect of curvature on C-F bonding in fluorinated carbons: from fullerene and derivates to graphite
W. Zhang, M. Dubois, K. Guérin, P. Bonnet, D. Claves, H. Kharbache, F. Masin, A.P. Kharitonov, A. Hamwi,
Phys. Chem. Chem. Phys., F.I.: 4,0600, 9999, Pekka Pyykkö

Articles publiés :

Effect of graphitization on fluorination of carbon nanocones and nanodiscs
W. Zhang, M. Dubois, K. Guérin, P. Bonnet, E. Petit, N. Delpuech, D. Albertini, F. Masin, A. Hamwi,
Carbon, F.I.: 4,373, 2009, P.A. Thrower, UK, Elsevier, 47 (12), 2763-2775
Télécharger version pdf
Solid state NMR study of carbon nanodiamonds produced by detonation technique
M. Dubois, K. Guérin, E. Petit, A. Hamwi, N. Komatsu, J. Giraudet, P. Pirotte, F. Masin
Journal of Physical Chemistry C, F.I.: 3,396, 2009, George C. Schatz, USA, ACS, Volume 113 (24), pages 10371-10378
Télécharger version pdf
Direct fluorination of carbon nanocones and nanodiscs
Z. Wei, L. Moch, M. Dubois, K. Guérin, J. Giraudet, F. Masin, A. Hamwi
Journal of Nanoscience and Nanotechnology, F.I.: 1,987, 2009, Hari Singh Nalwa, USA, ASP, Volume 9, pages 4496-4501
Télécharger version pdf
Carbon nanofibres fluorinated using TbF₄ as fluorinating agent Part II: adsorption and electrochemical properties
W. Zhang, K. Guérin, M. Dubois, A. Houdayer, F. Masin, A. Hamwi
Carbon, F.I.: 3,4190, 2008, P.A. Thrower, UK, Elsevier, 46 (7), 1017-1024
Télécharger version pdf
Solid state NMR and EPR study of fluorinated carbon nanofibres
Z. Wei, M. Dubois, K. Guérin, A. Hamwi, J. Giraudet, F. Masin
Journal of Solid State Chemistry, F.I.: 2,107, 2008, M. G. Kanatzidis, USA, Elsevier, Volume 181 (8), pages 1915-1924
Télécharger version pdf
First evidences of macroscopic orientation of benzene in C₆₀.4C₆H₆ solvate at 293 K.
F. Masin, A. S. Grell, M. Gelbcke, J. Giraudet
Solid State Communications, F.I.: 1,556, 2008, A. Pinczuk, UK, Elsevier, Volume 147 (2008), pages 49-52
Télécharger version pdf
Solid State NMR study of the post-fluorination of (C_2.5F)_n fluorine-GIC
J. Giraudet, M. Dubois, K. Guérin, C. Delabarre, A. Hamwi, F. Masin
Journal of Physical Chemistry B, F.I.: 4,115, 2007, George C. Schatz, USA, ACS, Volume 111, pages 14143-14151
Télécharger version pdf
Magnesium batteries: towards a first use of graphite fluoride
J. Giraudet, D. Claves, K. Guérin, M. Dubois, F. Masin, A. Hamwi
Journal of Power Sources, F.I.: 3,5200, 2007, C.K. Dyer, D.A.J. Rand, Z. Ogumi, B. Scrosati, P.T. Moseley, USA, Elsevier, Volume 173 (1), pages 592-598
Télécharger version pdf
Fluorinated Carbon Nanofibres for High Energy and High Power Densities Primary Lithium Batteries
R. Yazami, A. Hamwi, K. Guérin, M. Dubois, Y. Ozawa, J. Giraudet, F. Masin.
Electrochemistry Communications, F.I.: 3,388, 2007, R. G. Compton, UK, Elsevier, Volume 9 (7), pages 1850-1855
Télécharger version pdf
Heteronuclear dipolar recoupling using Hartmann-Hahn cross polarization: a probe for ¹⁹F-¹³C distance determination of fluorinated carbon materials
J. Giraudet, M. Dubois, K. Guérin, C. Delabarre, P. Pirotte, A. Hamwi, F. Masin
Solid State Nuclear Magnetic Resonance, F.I.: 1,4100, 2007, J. Klinowski, UK, Elsevier, Volume 31 (3), pages 131-140
Télécharger version pdf
Mineral control of carbon pools in a soil horizon
I. Basile-Doelsch, Amundson R., Stone W., Borscnheck D.,Bottero J. Y., Moustier S., Masin F. Colin F
Geoderma, F.I.: 1,7730, 15 January 2007, J.C. Bell, J. Chorover, A.E. Hartemink, A.B. McBratney, USA, Elsevier, Volume 137 (3-4), pages 477-489
Télécharger version pdf

Reactivity of Carbon Nanofibres with fluorine gas
F. Chamssedine, M. Dubois, K. Guérin, J. Giraudet, F. Masin, D.A. Ivanov, L. Vidal, R. Yazami, A. Hamwi
Chem. Mater., F.I.: 4,8180, 2007, Leonard V. Interrante, USA, ACS, 19 (2), 161-172
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Mesomorphism, Polymorphism, and Semicrystalline Morphology of Poly(Di-n-propylsiloxane)
R. I. Gearba, D. V. Anokhin, A. I. Bondar, Y. K. Godovsky, V. S. Papkov, N. N. Makarova, S. N. Magonov, W. Bras, M. H. J. Koch, F. Masin, B. Goderis and D. A. Ivanov
Macromolecules, F.I.: 4,0240, 2006, Timothy P. Lodge & associate, USA, ACS, 39 (3), 988-999
Télécharger version pdf
Solid State NMR studies of covalent graphite fluorides (CF)_n and (C₂F)_n.
J. Giraudet, M. Dubois, K. Guérin, A. Hamwi, F. Masin
Journal of Physics and Chemistry of Solids, F.I.: 1,4100, 2006, A. Bansil, K. Prassides, USA, Elsevier, 67 (5-6), 1100-1105
Télécharger version pdf
Comparative performances for primary lithium batteries of some covalent and semi-covalent graphite fluorides
J. Giraudet, C. Delabarre, K. Guérin, M. Dubois, F. Masin A. Hamwi,
Journal of Power Sources, F.I.: 2,7700, 2006, C.K. Dyer, D.A.J. Rand, Z. Ogumi, B. Scrosati, P.T. Moseley, USA, Elsevier, 158 (2), 1365-1372
Télécharger version pdf
EPR and solid-state NMR studies of poly(dicarbon monofluoride) (C₂F)_n
M. Dubois, J. Giraudet, K. Guérin, A. Hamwi, Z. Fawal, P. Pirotte, F. Masin
Journal of Physical Chemistry B, F.I.: 4,0330, 2006, George C. Schatz, USA, ACS, 110 (24), 11800-11808
Télécharger version pdf
Solid state NMR (¹⁹F and ¹³C) study of graphite monofluoride (CF)_n: ¹⁹F spin-lattice magnetic relaxation and ¹⁹F/¹³C distance determination by Hartmann-Hahn cross polarization
J. Giraudet, M. Dubois, A. Hamwi, W.E.E. Stone, P. Pirotte, F. Masin
Journal of Physical Chemistry B, F.I.: 4,0330, 2005, George C. Schatz, USA, ACS, 109 (1), 175-181
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Solid state ¹⁹F and ¹³C NMR of room temperature fluorinated graphite and samples thermally treated under fluorine: low field and high resolution studies
J. Giraudet, M. Dubois, K. Guérin, J.P. Pinheiro, A. Hamwi, W.E.E Stone, P. Pirotte, F. Masin;
Journal of Solid State Chemistry, F.I.: 1,7250, 2005, M.G. Kanatzidis, USA, Elsevier, 178 (4), 1262-1268
Télécharger version pdf

Mineralogical control of organic carbon dynamics in an volcanic ash soil on La Réunion
Basile-Doelsch, W. E. E. Stone, C. A. Masiello, J. Y. Bottero, F. Colin, F. Masin, D. Borscnheck and J. D. Meunier
European Journal of Soil Science, F.I.: 2,3560, 2005, P. Loveland, EU, Blackwell Publishing, 56 (6), 689-703
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Dynamical model for the C₅H₅ cycles in the C₆₀.2 ferrocene solvate
J. Rozen, R. Céolin, F. Masin
Physical review B, F.I.: 3,1850, 2004, P. D. Adams, USA, APS, 70, 144206 1-6
Télécharger version pdf

NMR and EPR studies of room temperature highly fluorinaded graphique heat-treated under fluorine atmosphere
M. Dubois, K. Guérin, J. P. Pinheiro, Z. Fawal, F. Masin, and A. Hamwi
Carbon, F.I.: 3,4190, 2004, P.A. Thrower, UK, Elsevier, 42 (10), 1931-1940
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Synthesis and characterization of Highly Fluorinated Graphite Containing sp² and sp³ Carbon
K. Guérin, J. P. Pinheiro, M. Dubois, Z. Fawal, F. Masin, R. Yazami, and A. Hamwi
Chem. Mater., F.I.: 4,8180, 2004, V. Leonard, USA, ACS, 16 (9), 1786-1792
Télécharger version pdf

Solid State ¹³C and ¹H NMR Investigations on C₆₀.2 ferrocene
J.Rozen, R. Céolin, J. L. Tamarit, H. Szwarc and F. Masin
Electronic properties of Novel Materials-Molecular Nanostructures, 2003, AIP, Kirchberg, Autriche, 19-22
Télécharger version pdf

A comparative X-ray diffraction, Mossbauer and NMR spectric study of the vermiculites from Béni Bousera, Morocoo and Palabora, Republic of South Africa.
Badreddine, R., Vandoermael, D., Fransolet, A.M., Long, G.J., Stone, W.E.E and Grandjean, F. (F. Masin = director)
Clay Minerals , F.I.: 1,1270, 2002, C. Derek, UK, The Clay Minerals Society, 37, 367-376

Phase Equilibria in the C₆₀ + Ferrocene system and Sodid-State Studies Of the C₆₀.2 Ferrocene Solvate,
P. Espeau, M. Barrio, D. O. Lopez, J. Li. Tamarit, R. Céolin, H. Allouchi, V. Agafonov, F. Masin, H. Szarc
Chem. Mater., F.I.: 4,8180, 2002, V. Leonard, USA, ACS, 14 (1), 321-326
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Molecular dynamics of C₇₀S₄₈ : dielectric function and nmr study
V. Talyzin, A.-S. Grell, F. Masin, A. B. Sherman, V. V. Lemanov, P. Lunkenheimer, R. Brand, A. Loidl
J. Phys. Chem. B, F.I.: 3,3950, 2001, M. A. El Sayed, USA, ACS, 105 (6), 1162-1167
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Speciation and Crystal Chemistry of Fe(III) Chloride Hydrolyzed in the Presence of SiO₄ Ligands.2.Characterization of Si-Fe Aggregates by FTIR and ²⁹Si Solid-State NMR.
Doelsch, E., Stone,W.E.E., Petit, P., Masion, A., Rose, J., Bottero, J.Y. and Nahon, D.(F. Masin = director)
Langmuir, F.I.: 3,1430, 2001, D. G. Whitten, USA, ACS, 17 (5), 1399-1405
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Le solvate C₆₀. 2S₈ : mystère et certitudes
H. Szwarc, A.-S. Grell, F. Masin, J.Ll. Tamarit, J.C. van Miltenburg, H. Allouchi, V. Agafonov, J. Rodriguez-Carvajal, R. Céolin
J. Phys. , F.I.: 1,9320, 2001, A. Paoletti, France, EDP Sciences, IV 11, 41-45

First NMR study on a C₆₀ ternary superconductor compound : (K₆C₆₀5C₆H₆)_1.5
A.-S. Grell, A. Hamwi, B. Berteaux, F. Masin
Electronic properties of Novel Materials-Molecular Nanostructures, 2000, AIP, IWEPNM2000 Int. Winterschool on Electronic Properties of Novels Materials, Kirchberg, Autriche, 42-45
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Retention of zinc and chromium ions by different phases of hydrated calcium aluminate: a solid-state ²⁷Al NMR study.
Moulin,I., Stone,W.E.E., Sanz,J., Bottero,J.Y., Mosnier,F. and Haehnel,C. (F. Masin = Director)
J. Phys. Chem. B, F.I.: 3,3950, 2000, M. A. El Sayed, USA, ACS, 104 (39), 9230-9238

Tautomerism in Schiff bases derived from 3-hydroysalicylaldehyde. Combined x-ray diffraction, solution and solid-state NMR study.
Pizzala,H., Carles,M., Stone,W.E.E. and Thevand,A.(F. Masin = director)
J. Chem. Soc. Perkin Trans. 2, F.I.: 1,6000, 2000, Royal Society of Chemistry, Burlington House, Rodney Townsend, 5, 935-939

Tautomeric polymorphism in salicylideneamine derivatives: an x-ray diffraction and solid-state NMR study.
Pizzala,H., Carles,M., Stone,W.E.E. and Thevand,A.(F. Masin = director)
J. Molecular Structure , 2000, A.J. Barnes, Texas A&M University, College Station, Texas, Elsevier, 526, 261-268

Molecular dynamics of C₆₀.2S₈ : a ¹³C NMR study
A.-S. Grell, F. Masin, R. Céolin, M.-F. Gardette, and H. Szwarc
Phys. Rev. B, F.I.: 2,8340, 2000, P. D. Adams, USA, APS, 62 (6), 3722-3726

The NMR answer to the anomalous solubility behaviour of fullerenes
R.J. Doome, A.-S. Grell, F. Masin, A. Fonseca, J.B. Nagy
Molecular Materials vol 13, 2000, St Petersbourg, Russie, 3

Structural and dynamics characterization of benzene-solvated C₆₀ studied by NMR
I. Messari, A.-S. Grell, R. Doome, J.B. Nagy, P. Tekely, and F. Masin
Molecular Materials vol 13, 2000, St Petersbourg, Russie, 3

Molecular dynamics study of C₆₀.2S₈ by ¹³C NMR
A.-S. Grell, R. Céolin, M.-F. Gardette, H. Szwarc, and F. Masin
Molecular Materials Vol 13, 2000, St Petersbourg, Russie, 3

Communications Orales:

New synthesis methods for fluorinated carbon nanofibres”
Wei Zhang, Marc Dubois, Katia Guérin, Hayat Kharbache, Francis Masin, André Hamwi,
CARBON 2009, June 14-19, 2009, Biarritz, France
Fluorination of nanocarbons using fluorinating agent
Wei Zhang, Marc Dubois, Katia Guérin, Pierre Bonnet, Francis Masin, André Hamwi,
E-MRS 2009 Spring Meeting , June 8 - 12, 2009, Strasbourg, France
C-F bonding into fluorinated nanocarbons
Marc Dubois, Wei Zhang, , Katia Guérin, Hayat Kharabache, A.P. Kharitonov, André Hamwi, Francis Masin,
NanoteC , August 26th – 29th, 2009, Bruxelles, Belgique
Fluorination of carbon nanocones and nanodiscs
W. Zhang, M. Dubois, K. Guérin, A. Hamwi, J. Giraudet, F. Masin
Carbon 2008, Nagano (Japon), 13-18 juillet 2008
New fluorinated carbons for energy storage
M. Dubois, W. Zhang, K. Guerin, J. Giraudet, F. Masin, R. Yazami, A. Hamwi
Carbon 2008, Nagano (Japon), 13-18 juillet 2008
Solid state NMR studies of covalent graphite fluorides (CF)_n and (C₂F)_n.
J. Giraudet, M. Dubois, K. Guerin, A. Hamwi, F. Masin
13th International Symposium of Intercalation Compounds, Clermont Ferrand, 6-9 Juin 2005 (Conférence internationale)
Solid State NMR and EPR studies of fluorinated graphites.
M. Dubois, J. Giraudet, K. Guerin, C. Delabarre, Z. Fawal, A. Hamwi, F. Masin
17th International Symposium on Fluorine Chemistry, Shanghai, Chine, 24-29 Juillet 2005 (Conférence internationale)
La RMN ¹⁹F et ¹³C comme outil de caractérisation des carbones fluorés.
J. Giraudet, M. Dubois, K. Guerin, A. Hamwi, F. Masin
9ème Réunion de Travail RMN du Solide d'Eveux, La Baume, 27-30 Novembre 2006
Versatility of the C-F bonding into fluorinated carbons.
M. Dubois, J. Giraudet, K. Guerin, W. Zhang, D. Claves, A. Hamwi, F. Masin
Japanese-French Seminar on Fluorine Chemistry, Reims, France, 11-13 Juillet 2007 (Conférence internationale)
Fluorination of carbon nanofibres using fluorinating reagent.
A. Hamwi, W. Zhang, M. Dubois, K. Guerin, J. Giraudet, F. Masin
CARBON 2007, Seattle, USA, 15-20 Juillet 2007 (Conférence internationale)

Affiches:

Solid state NMR study of fluorinated fullerenes
W. Zhang, M. Dubois, D. Claves, K. Guérin, P. Pirotte, F. Masin, J. Giraudet, A. Hamwi,
CARBON 2009, June 14-19, 2009, Biarritz, France
Solid State NMR study of nanodiamonds produced by various techniques
N. Batisse, M. Dubois, K. Guérin, E. Petit, A. Hamwi, N. Komatsu, J. Giraudet, P. Pirotte, H. Kharbache, F. Masin,
CARBON 2009, June 14-19, 2009, Biarritz, France
Fluorination of nanodiscs and nanocones
W. Zhang, M. Dubois, K. Guérin, P. Bonnet, H. Kharabache, F. Masin, A. Hamwi,
NanoteC , August 26th – 29th, 2009, Bruxelles, Belgique
Fluorination of nanodiscs and nanocones
W. Zhang, M. Dubois, K. Guérin, P. Bonnet, H. Kharabache, F. Masin, A. Hamwi,
The International Conference on Fluorine Chemistry '09 Kyoto, 20-22 May 2009, Kyoto, Japan.
Solid State NMR study of carbon nanodiamonds produced by detonation technique
N. Komatsu, M. Dubois, K. Guérin, A. Hamwi, J. Giraudet, P. Pirotte, F. Masin
Carbon 2009, Nagano (Japon), 15 May 2009
Performances comparées de piles au lithium pour quelques fluorures de graphite.
J. Giraudet, K. Guerin, M. Dubois, C. Delabarre, F. Masin, A. Hamwi
Groupe Français d'Etude des Composés d'Insertion, Aubière, 9-10 Juin 2005
Hartmann-Hahn cross polarization: a probe for ¹⁹F-¹³C distance determination of fluorinated carbon materials.
J. Giraudet, M. Dubois, K. Guerin, Z. Fawal, A. Hamwi, F. Masin
Carbon 2006, Aberdeen, Ecosse, 16-21 Juillet 2006 (Conférence internationale)
EPR and solid state NMR studies of poly(dicarbon monofluoride) (C₂F)_n: effects of physisorbed oxygen.
M. Dubois, J. Giraudet, K. Guerin, A. Hamwi, P. Pirotte, F. Masin
18th International Symposium on Fluorine Chemistry, University of Bremen, Allemagne, 30 Juillet – 4 Aout 2006 (Conférence internationale)
Versatility of the C-F bonding into fluorinated carbons: ¹⁹F-¹³C distance determination using NMR.
J. Giraudet, M. Dubois, K. Guerin, W. Zhang, D. Claves, A. Houdayer, P. Pirotte, A. Hamwi, F. Masin
15th European Symposium on Fluorine Chemistry, Prague, République Tchèque, 15-20 Juillet, 2007 (Conférence internationale)
Fluorination of carbon nanofibres: fluorine gas vs fluorinating reagent.
W. Zhang, M. Dubois, K. Guerin, A. Houdayer, J. Giraudet, F. Masin, A. Hamwi
15th European Symposium on Fluorine Chemistry, Prague, République Tchèque, 15-20 Juillet, 2007 (Conférence internationale)
Fluorination of carbon nanofibres: fluorine gas vs fluorinating reagent.
W. Zhang, M. Dubois, K. Guerin, A. Hamwi, J. Giraudet, F. Masin, A. Houdayer
Carbon for Energy Storage and Environment Protection 07, Krakow, Pologne, 2-6 Septembre, 2007 (Conférence internationale)

Spectre WISE du PDPS (C-H)

Thèses et mémoires :

Etude de la dynamique moléculaire du poly(di-n-propylsiloxane) par RMN en phase anisotrope
Mémoire (Télécharger version pdf)
Présentation (Télécharger version pdf)
Présentation (Télécharger version ppt)
A. Walter (mémoire 2006-2007)

Etude de la dynamique moléculaire du complexe C₆₀(ferrocène)₂ par RMN en phase solide
A. Scollier (mémoire 2005-2006 )

Résonance Magnétique Nucléaire (RMN) du solide : Dynamique moléculaire et mécanisme de relaxation dans le fluorure de graphite covalent (CF)_n, Etude à bas champ, en ¹⁹F MAS et ¹⁹F-¹³C CP-MAS de fluorures de graphite ionique CF_x(IF₅)_yRapport (Télécharger version pdf)
J. Giraudet (post doct. 2002-2003)

Thèse de doctorat en science de Monsieur J. Rozen
(depuis 2002)

Détermination de la dynamique moléculaire d'une poudre de C₆₀.2CCl₄A. Ben Ahmed (mémoire 2001-2002)

Etude de la dynamique moléculaire en phase solide du solvaté C₆₀. 2 ferrocènes
J. Rozen (mémoire 2001-2002)

Thèse de doctorat en science de Madame A.-S. Grell
(défendue en 2001)